PEM5148 - Electrochemistry applied to materials
Form professor
Prof. Dr. Celia Regina Tomachuk dos Santos Catuogno
Workload
| Theoretical |
Practical |
Study |
Duration |
Total |
Credits |
| 4 hours/week |
0 hours/week |
8 hours/week |
15 weeks |
180 hours |
12 |
See on Janus (pt-br)
Concentration area
97135 - Conventional and Advanced Materials
Objectives
To provide to the studentes the fundamentals on electrochemical characterization in probe scanning techniques and electrochemical impedance spectroscopy.
Motivation
The interpretation of voltmmograms and impedance diagrams will be correlated with observed behavior in electrochemical interfaces, and may be associated with corrosion and protection.
Syllabus
- Electrochemical Characterization: Voltammetric Techniques; Amperometric and Electroanalytical Techniques
- Scanning Probe Techniques: Applications Electrochemistry and Electrochemical Microscopy
- Electrochemical Impedance Spectroscopy
Evaluation criteria
an oral presentation (weight 1) and a written exam (weight 2).
References
- BARD A.J.; FAULKNER L.R. Electrochemical Methods:Fundamentals and Applications. New York: John Wiley & Sons, 2ª Edição, 2011, 864p
- BAGOTTZKY V. S. Fundamentals of Electrochemistry. New York: John Wiley & Sons, 2ª Edição, 2005, 752p
- BARSOUKOV E.; MACDONALD J.R. Impedance Spectroscopy: Theory, Experiment, and Applications. New Jersey: John Wiley & Sons, 2ª Edição, 2005, 616p.
- BOCKRIS J. O’M.; REDDY A.K.N.; GAMBOA-ALDECO A.M. Modern electrochemistry. New York: Kluwer Academic Publishers, 2ª Edição, vol 2A, 2002.
- BRETT A.M.O.; BRETT C.M.A. Electroquímica: Princípios, Métodos e Aplicações. Coimbra: Livraria Almedina, 1993, 471p.
- CROW D.R. Principles and Applications of Electrochemistry. London: CRC Press, 4ª Edição, 1996, 282p.
- GILEADI E. Physical Electrochemistry: Fundamentals, Techniques and Applications. New York: Wiley-VCH, 2011, 394p.
- GROSSER-Jr, D.K. Cyclic voltammetry: simulation and analysis of reactions mechanisms. New York: Wiley-VCH,1993, 156p.
- SCULLY J.R.; SILVERMAN D.C.; KENDIG M.W. Electrochemical impedance: analysis and interpretation. Philadelphia, ASTM, 1993, 480 p.
- TICIANELLI E.A.; GONZÁLEZ E.R. Eletroquímica, Princípios e Aplicações. São Paulo: Editora da Universidade de São Paulo, 2ª Edição, 2005. 220p.
- WOLYNEC S. Técnicas Eletroquímicas em Corrosão. São Paulo: Editora da Universidade de São Paulo, 2003. 166p.
- Análise de artigos atuais das revistas Electrochimica Acta, J. Applied Electrochemistry e Surface Coating Techonology